Benchtop flow-NMR for rapid online monitoring of RAFT and free radical polymerisation in batch and continuous reactors

Stephen T. Knox; Sam Parkinson; Raphael Stone; Nicholas J. Warren

doi:10.1039/c9py00982e

Benchtop flow-NMR for rapid online monitoring of RAFT and free radical polymerisation in batch and continuous reactors

Stephen T. Knox
, Sam Parkinson
, Raphael Stone
, Nicholas J. Warren

Research output: Contribution to journal › Article › peer-review

54 Citations (SciVal)

Abstract

A “Benchtop” NMR spectrometer is used for detailed monitoring of controlled and free radical polymerisations performed in batch and continuous reactors both offline and in real-time. This allows detailed kinetic analysis with unprecedented temporal resolution for reactions which reach near completion in under five minutes.

A “Benchtop” NMR spectrometer is used for detailed monitoring of controlled and free radical polymerisations performed in batch and continuous reactors both offline and in real-time.

Original language	English
Pages (from-to)	4774-4778
Number of pages	5
Journal	Polymer Chemistry
Volume	10
Issue number	35
Early online date	7 Aug 2019
DOIs	https://doi.org/10.1039/c9py00982e
Publication status	Published - Sept 2019

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title = "Benchtop flow-NMR for rapid online monitoring of RAFT and free radical polymerisation in batch and continuous reactors",

abstract = "A “Benchtop” NMR spectrometer is used for detailed monitoring of controlled and free radical polymerisations performed in batch and continuous reactors both offline and in real-time. This allows detailed kinetic analysis with unprecedented temporal resolution for reactions which reach near completion in under five minutes.A “Benchtop” NMR spectrometer is used for detailed monitoring of controlled and free radical polymerisations performed in batch and continuous reactors both offline and in real-time.",

author = "Knox, \{Stephen T.\} and Sam Parkinson and Raphael Stone and Warren, \{Nicholas J.\}",

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AU - Knox, Stephen T.

AU - Parkinson, Sam

AU - Stone, Raphael

AU - Warren, Nicholas J.

PY - 2019/9

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N2 - A “Benchtop” NMR spectrometer is used for detailed monitoring of controlled and free radical polymerisations performed in batch and continuous reactors both offline and in real-time. This allows detailed kinetic analysis with unprecedented temporal resolution for reactions which reach near completion in under five minutes.A “Benchtop” NMR spectrometer is used for detailed monitoring of controlled and free radical polymerisations performed in batch and continuous reactors both offline and in real-time.

AB - A “Benchtop” NMR spectrometer is used for detailed monitoring of controlled and free radical polymerisations performed in batch and continuous reactors both offline and in real-time. This allows detailed kinetic analysis with unprecedented temporal resolution for reactions which reach near completion in under five minutes.A “Benchtop” NMR spectrometer is used for detailed monitoring of controlled and free radical polymerisations performed in batch and continuous reactors both offline and in real-time.

UR - https://pubs.rsc.org/en/content/articlelanding/2019/py/c9py00982e

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DO - 10.1039/c9py00982e

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SP - 4774

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JO - Polymer Chemistry

JF - Polymer Chemistry

IS - 35

ER -

Benchtop flow-NMR for rapid online monitoring of RAFT and free radical polymerisation in batch and continuous reactors

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